Preparation of Iron Nanoparticles from Iron Pentacarbonyl Using an Atmospheric Microwave Plasma

ZHANG Boya (张博雅); WANG Qiang (王强); ZHANG Guixin (张贵新); LIAO Shanshan (廖姗姗); WANG Zhong (王仲); LI Guobin (李国斌)

doi:10.1088/1009-0630/17/10/11

Plasma Science and Technology > 2015 > 17(10): 876-880. > DOI: 10.1088/1009-0630/17/10/11

ZHANG Boya (张博雅), WANG Qiang (王强), ZHANG Guixin (张贵新), LIAO Shanshan (廖姗姗), WANG Zhong (王仲), LI Guobin (李国斌). Preparation of Iron Nanoparticles from Iron Pentacarbonyl Using an Atmospheric Microwave Plasma[J]. Plasma Science and Technology, 2015, 17(10): 876-880. DOI: 10.1088/1009-0630/17/10/11

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Preparation of Iron Nanoparticles from Iron Pentacarbonyl Using an Atmospheric Microwave Plasma

1Department of Electrical Engineering, Tsinghua University, Beijing 100084, China 2Shenzhen Power Supply Co. Ltd., Shenzhen 518000, China 3North Institute of Material Science and Engineering, Ningbo 315103, China

Funds: supported by National Natural Science Foundation of China (No. 51177085), the State Key Laboratory Foundation of Power System of China (No. SKLD10M07) and China Postdoctoral Science Foundation (No. 2013M540942)

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Received Date: December 24, 2014

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Abstract

Abstract

A novel method is introduced for preparing iron nanoparticles from iron pentacar?bonyl using an atmospheric microwave plasma. The prepared iron nanoparticles were characterized by transmission electron microscopy and X-ray diffraction. The results show that the size of the particles can be controlled by adjusting the microwave power and the flow rate of the carrier gas. The magnetic properties of the synthesized iron particles were studied and a saturation magnetiza?tion of ～95 emu/g was obtained. The convenient preparation process and considerable production rate were also found to be satisfactory for industrial applications.
- microwave plasma,
- nanoparticles,
- iron pentacarbonyl,
- magnetic materials

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