Development of a Laboratory Cement Quality Analysis Apparatus Based on Laser-Induced Breakdown Spectroscopy

FAN Juanjuan (樊娟娟); ZHANG Lei (张雷); WANG Xin (王鑫); LI Yufang (李郁芳); GONG Yao (弓瑶); DONG Lei (董磊); MA Weiguang (马维光); YIN Wangbao (尹王保); WANG Zhe (王哲); LI Zheng (李政); ZHANG Xiangjie (张向杰); LI Yi (李逸); JIA Suotang (贾锁堂)

doi:10.1088/1009-0630/17/11/01

Plasma Science and Technology > 2015 > 17(11): 897-903. > DOI: 10.1088/1009-0630/17/11/01

FAN Juanjuan (樊娟娟), ZHANG Lei (张雷), WANG Xin (王鑫), LI Yufang (李郁芳), GONG Yao (弓瑶), DONG Lei (董磊), MA Weiguang (马维光), YIN Wangbao (尹王保), WANG Zhe (王哲), LI Zheng (李政), ZHANG Xiangjie (张向杰), LI Yi (李逸), JIA Suotang (贾锁堂). Development of a Laboratory Cement Quality Analysis Apparatus Based on Laser-Induced Breakdown Spectroscopy[J]. Plasma Science and Technology, 2015, 17(11): 897-903. DOI: 10.1088/1009-0630/17/11/01

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Development of a Laboratory Cement Quality Analysis Apparatus Based on Laser-Induced Breakdown Spectroscopy

1State Key Laboratory of Quantum Optics and Quantum Optics Devices, Institute of Laser Spectroscopy, Shanxi University, Taiyuan 030006, China 2State Key Lab of Power Systems, Department of Thermal Engineering, Tsinghua-BP Clean Energy Center, Tsinghua University, Beijing 100083, China 3Taiyuan Amethyst Technology Co., Ltd., Taiyuan 030006, China 4Shanxi Zhongtiaoshan New Building Materials Co., Ltd., Linfen 041000, China

Funds: supported by National Natural Science Foundation of China (Nos. 61127017,61378047, 61205216, 61178009, 61108030,61475093, and 61275213), the National Key Technology R&D Program of China (No. 2013BAC14B01), the 973 Program of China (No. 2012CB921603), the Shanxi Natural Science Foundation, China (Nos. 2013021004-1, 2012021022-1), and the Shanxi Scholarship Council of China (Nos. 2013-011 and 2013-01)

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Received Date: April 20, 2015

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Abstract

Abstract

Determination of the chemical composition of cement and ratio values of clinker plays an important role in cement plants as part of the optimal process control and product quality evaluation. In the present paper, a laboratory laser-induced breakdown spectroscopy (LIBS) apparatus mainly comprising a sealed optical module and an analysis chamber has been designed for possible application in cement plants for on-site quality analysis of cement. Emphasis is placed on the structure and operation of the LIBS apparatus, the sealed optical path, the temperature controlled spectrometer, the sample holder, the proper calibration model established for minimizing the matrix effects, and a correction method proposed for overcoming the ‘drift’ obstacle. Good agreement has been found between the laboratory measurement results from the LIBS method and those from the traditional method. The absolute measurement errors presented here for oxides analysis are within 0.5%, while those of ratio values are in the range of 0.02 to 0.05. According to the obtained results, this laboratory LIBS apparatus is capable of performing reliable and accurate, composition and proximate analysis of cement and is suitable for application in cement plants.
- laser-induced breakdown spectroscopy,
- LIBS,
- cement,
- composition analysis,
- proximate analysis,
- ratio values,
- linear correction method

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References

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