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FAN Juanjuan (樊娟娟), ZHANG Lei (张雷), WANG Xin (王鑫), LI Yufang (李郁芳), GONG Yao (弓瑶), DONG Lei (董磊), MA Weiguang (马维光), YIN Wangbao (尹王保), WANG Zhe (王哲), LI Zheng (李政), ZHANG Xiangjie (张向杰), LI Yi (李逸), JIA Suotang (贾锁堂). Development of a Laboratory Cement Quality Analysis Apparatus Based on Laser-Induced Breakdown Spectroscopy[J]. Plasma Science and Technology, 2015, 17(11): 897-903. DOI: 10.1088/1009-0630/17/11/01
Citation: FAN Juanjuan (樊娟娟), ZHANG Lei (张雷), WANG Xin (王鑫), LI Yufang (李郁芳), GONG Yao (弓瑶), DONG Lei (董磊), MA Weiguang (马维光), YIN Wangbao (尹王保), WANG Zhe (王哲), LI Zheng (李政), ZHANG Xiangjie (张向杰), LI Yi (李逸), JIA Suotang (贾锁堂). Development of a Laboratory Cement Quality Analysis Apparatus Based on Laser-Induced Breakdown Spectroscopy[J]. Plasma Science and Technology, 2015, 17(11): 897-903. DOI: 10.1088/1009-0630/17/11/01

Development of a Laboratory Cement Quality Analysis Apparatus Based on Laser-Induced Breakdown Spectroscopy

Funds: supported by National Natural Science Foundation of China (Nos. 61127017,61378047, 61205216, 61178009, 61108030,61475093, and 61275213), the National Key Technology R&D Program of China (No. 2013BAC14B01), the 973 Program of China (No. 2012CB921603), the Shanxi Natural Science Foundation, China (Nos. 2013021004-1, 2012021022-1), and the Shanxi Scholarship Council of China (Nos. 2013-011 and 2013-01)
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  • Received Date: April 20, 2015
  • Determination of the chemical composition of cement and ratio values of clinker plays an important role in cement plants as part of the optimal process control and product quality evaluation. In the present paper, a laboratory laser-induced breakdown spectroscopy (LIBS) apparatus mainly comprising a sealed optical module and an analysis chamber has been designed for possible application in cement plants for on-site quality analysis of cement. Emphasis is placed on the structure and operation of the LIBS apparatus, the sealed optical path, the temperature controlled spectrometer, the sample holder, the proper calibration model established for minimizing the matrix effects, and a correction method proposed for overcoming the ‘drift’ obstacle. Good agreement has been found between the laboratory measurement results from the LIBS method and those from the traditional method. The absolute measurement errors presented here for oxides analysis are within 0.5%, while those of ratio values are in the range of 0.02 to 0.05. According to the obtained results, this laboratory LIBS apparatus is capable of performing reliable and accurate, composition and proximate analysis of cement and is suitable for application in cement plants.
  • 1 Aldridge L P. 1982, Cement and Concrete Research,12: 437 2 Li L Z, Wang Z, Yuan T B, et al. 2011, Journal of Analytical Atomic Spectrometry, 26: 2274 3 Dong M R, Lu J D, Yao S C, et al. 2011, Journal of Analytical Atomic Spectrometry, 26: 2183 4 Wang Z, Li Z, West L, et al. 2012, Spectrochimica Acta Part B, 68: 58 5 Wang Z, Yuan T B, Hou Z Y, et al. 2014, Frontiers of Physics, 9: 419 6 Wang Q Q, Liu K, Zhao H, et al. 2012, Frontiers of Physics, 7: 701 7 Cai Y, Chu P C, Ho S K, et al. 2012, Frontiers of Physics, 7: 670 8 Wang Z, Yuan T B, Lui S L, et al. 2012, Frontiers of Physics, 7: 708 9 Gondal A, Dastageer A, Maslehuddin M, et al. 2012,Optics and Laser Technology, 44: 566 10 Timur A L, Andrey M P, Sergey M Z, et al. 2014,Spectrochimica Acta Part B, 99: 94 11 Weritz F, Ryahi S, Schaurich D, et al. 2005, Spectrochimica Acta Part B, 60: 1121 12 Christoph D G, Eugen W, Reinhard N, et al. 2009,Spectrochimica Acta Part B, 64: 1135 13 Mansoori A, Roshanzadeh B, Khalaji M, et al. 2011,Optics and Lasers in Engineering, 49: 318 14 Li X F, Zhou W D, Li K X, et al. 2012, Optics Communications, 285: 54 15 Zhou W D, Su X J, Qian H G, et al. 2013, Journal of Analytical Atomic Spectrometry, 28: 702 16 Zhang L, Dong L, Dou H P, et al. 2008, Applied Spectroscopy, 62: 458 17 Ko J B, Sdorra W, Niemax K. 1989, Journal of Analytical Chemistry, 335: 648 18 Kanicky V, Mermet J M. 1996, Journal of Analytical Chemistry, 355: 887 19 Dong F Z, Chen X L, Wang Q, et al. 2012, Frontiers of Physics, 7: 679 20 Zhang L, Ma W G, Dong L, et al. 2011, Applied Spectroscopy, 65: 790
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