Elemental analysis of copper alloy by high repetition rate LA-SIBS using compact fiber spectrometer

Xiaoyong HE (何小勇); Runhua LI (李润华); Fujuan WANG (王福娟)

doi:10.1088/2058-6272/aae1f1

Plasma Science and Technology > 2019 > 21(3): 34005-034005. > DOI: 10.1088/2058-6272/aae1f1

Xiaoyong HE (何小勇), Runhua LI (李润华), Fujuan WANG (王福娟). Elemental analysis of copper alloy by high repetition rate LA-SIBS using compact fiber spectrometer[J]. Plasma Science and Technology, 2019, 21(3): 34005-034005. DOI: 10.1088/2058-6272/aae1f1

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Elemental analysis of copper alloy by high repetition rate LA-SIBS using compact fiber spectrometer

¹ School of Physics and Optoelectronics, South China University of Technology, Guangzhou 510641, People’s Republic of China
² State Key Laboratory of Optoelectronic Materials and Technology, Sun Yat-sen University, Guangzhou 510275, People’s Republic of China

Funds: This work was financially supported by National Basic Research Program (973 Program) of China under grant number 2012CB921900 and National Natural Science Foundation of China under grant numbers 11274123 and 11304100.

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Received Date: June 06, 2018

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Abstract

Abstract

High repetition rate laser-ablation spark-induced breakdown spectroscopy (HRR LA-SIBS) was first used to analyze trace elements in copper alloy samples. The 1064 nm output of an acousto- optically Q-switched Nd:YAG laser operated at a pulse repetition rate of 1 kHz was utilized to ablate copper alloy and to form original plasma, spark-discharge was applied to further breakdown the ablated samples and enhance the emission of the laser-induced plasma. A compact multichannel fiber spectrometer was used to analyze the plasma emission under non- gated operation mode. Under the assistance of high repetition rate spark discharge, the plasma emission was able to be improved significantly. The determined limits of the detection of lead and aluminum were 15.5 ppm and 1.9 ppm by HRR LA-SIBS, respectively, which were 11 and 6 folds better than that determined by HRR LIBS under the same laser-ablation condition. This work demonstrates the feasibility of using fiber spectrometer to analyze plasma emission under non-gated operation mode and the possibility of building a portable HRR LA-SIBS system for rapid elemental analysis of copper alloys and other solid samples.
- high repetition rate,
- laser-ablation spark-induced breakdown spectroscopy,
- copper alloy,
- rapid analysis

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References (36)

References

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Elemental analysis of copper alloy by high repetition rate LA-SIBS using compact fiber spectrometer