Surface treatment of titanium dioxide nanopowder using rotary electrode dielectric barrier discharge reactor

Naw Rutha PAW; Takuma KIMURA; Tatsuo ISHIJIMA; Yasunori TANAKA; Yusuke NAKANO; Yoshihiko UESUGI; Shiori SUEYASU; Shu WATANABE; Keitaro NAKAMURA

doi:10.1088/2058-6272/ac0ed9

Plasma Science and Technology > 2021 > 23(10): 105505. > DOI: 10.1088/2058-6272/ac0ed9

Naw Rutha PAW, Takuma KIMURA, Tatsuo ISHIJIMA, Yasunori TANAKA, Yusuke NAKANO, Yoshihiko UESUGI, Shiori SUEYASU, Shu WATANABE, Keitaro NAKAMURA. Surface treatment of titanium dioxide nanopowder using rotary electrode dielectric barrier discharge reactor[J]. Plasma Science and Technology, 2021, 23(10): 105505. DOI: 10.1088/2058-6272/ac0ed9

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Surface treatment of titanium dioxide nanopowder using rotary electrode dielectric barrier discharge reactor

¹ Faculty of Electrical Engineering and Computer Science, Kanazawa University, Kanazawa 920-1192, Japan
² Research Center for Production & Technology, Nisshin Seifun Group Inc., Fujimino 356-8511, Japan

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Received Date: April 21, 2021
Revised Date: June 17, 2021
Accepted Date: June 26, 2021

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Abstract

Abstract

Titanium dioxide (TiO₂) nanopowder (P-25; Degussa AG) was treated using dielectric barrier discharge (DBD) in a rotary electrode DBD (RE-DBD) reactor. Its electrical and optical characteristics were investigated during RE-DBD generation. The treated TiO₂ nanopowder properties and structures were analyzed using x-ray diffraction (XRD) and Fourier-transform infrared spectroscopy (FTIR). After RE-DBD treatment, XRD measurements indicated that the anatase peak theta positions shifted from 25.3° to 25.1°, which can be attributed to the substitution of new functional groups in the TiO₂ lattice. The FTIR results show that hydroxyl groups (OH) at 3400 cm⁻¹ increased considerably. The mechanism used to modify the TiO₂ nanopowder surface by air DBD treatment was confirmed from optical emission spectrum measurements. Reactive species, such as OH radical, ozone and atomic oxygen can play key roles in hydroxyl formation on the TiO₂ nanopowder surface.
- dielectric barrier discharge,
- nanopowder,
- reactive species,
- rotary electrodes,
- surfacetreatment,
- titanium dioxide

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Surface treatment of titanium dioxide nanopowder using rotary electrode dielectric barrier discharge reactor