The comparison of manganese spectral lines for self-absorption reduction in LIBS using laser-induced fluorescence

Yun TANG; Jingfeng LI; Shixiang MA; Zhenlin HU; Xuxiang PENG; Weiping ZHOU; Xiao YUAN; Meng SHEN

doi:10.1088/2058-6272/acb24f

Plasma Science and Technology > 2023 > 25(6): 065505. > DOI: 10.1088/2058-6272/acb24f

Yun TANG, Jingfeng LI, Shixiang MA, Zhenlin HU, Xuxiang PENG, Weiping ZHOU, Xiao YUAN, Meng SHEN. The comparison of manganese spectral lines for self-absorption reduction in LIBS using laser-induced fluorescence[J]. Plasma Science and Technology, 2023, 25(6): 065505. DOI: 10.1088/2058-6272/acb24f

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The comparison of manganese spectral lines for self-absorption reduction in LIBS using laser-induced fluorescence

1.
Hunan Province Key Laboratory of Intelligent Sensors and Advanced Sensor Materials, School of Physics and Electronic Science, Hunan University of Science and Technology, Xiangtan 411201, People's Republic of China
2.
National Engineering Research Center of Intelligent Equipment for Agriculture, Beijing Academy of Agriculture and Forestry Sciences, Beijing 100097, People's Republic of China
3.
Wuhan National Laboratory for Optoelectronics (WNLO), Huazhong University of Science and Technology, Wuhan 430074, People's Republic of China

More Information

Corresponding author:
Yun TANG, E-mail: yuntang@hnust.edu.cn

Meng SHEN, E-mail: josephshen@hust.edu.cn
Received Date: November 13, 2022
Revised Date: January 08, 2023
Accepted Date: January 10, 2023
Available Online: December 05, 2023
Published Date: March 13, 2023

Graphical Abstract

Abstract

Abstract

The detection of manganese (Mn) in steel by laser-induced breakdown spectroscopy (LIBS) provides essential information for steelmaking. However, self-absorption greatly disrupts the LIBS spectral lines of Mn with high content. In this study, to minimize self-absorption for Mn spectral lines in LIBS, laser-induced fluorescence (LIF) was applied. Compared with conventional LIBS, the self-absorption factors (α) of Mn I 403.08, 403.31, and 403.45 nm lines were reduced by 90%, 88%, and 88%, respectively; the root mean square errors of cross-validation were decreased by 88%, 85%, and 87%, respectively; the average relative errors were reduced by 93%, 90%, and 91%, respectively; and average relative standard deviations were decreased by 29%, 32%, and 33%, respectively. The LIBS-LIF was shown to successfully minimize the self-absorption effect and spectral intensity fluctuation and improve detection accuracy.
- laser-induced breakdown spectroscopy,
- self-absorption,
- LIBS-LIF

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Acknowledgments

This research was financially supported by National Natural Science Foundation of China (No. 62005078), the Scientific Research Foundation of Hunan Provincial Education Department (No. 21B0477), and the Natural Science Foundation of Hunan Province (No. 2020JJ5206).

References (26)

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The comparison of manganese spectral lines for self-absorption reduction in LIBS using laser-induced fluorescence

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