An efficient procedure in quantitative analysis using laser-induced breakdown spectroscopy

Congyuan PAN (潘从元); Jiao HE (何娇); Guangqian WANG (王广谦); Xuewei DU (杜学维); Yongbin LIU (刘永斌); Yahui SU (苏亚辉)

doi:10.1088/2058-6272/aaf50f

Plasma Science and Technology > 2019 > 21(3): 34012-034012. > DOI: 10.1088/2058-6272/aaf50f

Congyuan PAN (潘从元), Jiao HE (何娇), Guangqian WANG (王广谦), Xuewei DU (杜学维), Yongbin LIU (刘永斌), Yahui SU (苏亚辉). An efficient procedure in quantitative analysis using laser-induced breakdown spectroscopy[J]. Plasma Science and Technology, 2019, 21(3): 34012-034012. DOI: 10.1088/2058-6272/aaf50f

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An efficient procedure in quantitative analysis using laser-induced breakdown spectroscopy

¹ College of Electrical Engineering and Automation, Anhui University, Hefei 230601, People’s Republic of China
² National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei 230029, People’s Republic of China

Funds: The authors are grateful for the financial support provided by National Natural Science Foundation of China (11704372) and Anhui Provincial Natural Science Foundation (1708085QF130).

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Received Date: July 29, 2018

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Abstract

Abstract

Laser-induced breakdown spectroscopy has become a general-purpose technique, and internal standard calibration is a common method for quantitative analysis. Calibration models should be reconstructed for different systems and application environments. This study presents an efficient procedure in the construction and selection of calibration models for LIBS analysis. The procedure concludes data preprocess, calibration model construction, and concentration calculation. These steps can be programmed without manual intervention. Results of the quantitative analysis of Ni-based alloys using the proposed procedure are presented in this study. Ten elements are calibrated, and most have an average relative standard error of less than 10%. The proposed procedure is an effective process for constructing and selecting calibration models.
- laser-induced breakdown spectroscopy,
- quantitative analysis,
- procedure,
- alloys

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An efficient procedure in quantitative analysis using laser-induced breakdown spectroscopy