
Citation: | Sai SRIKAR, Tinku KUMAR, Degala Venkata KIRAN, Reetesh Kumar GANGWAR. Non-invasive optical characterization and estimation of Zn porosity in gas tungsten arc welding of Fe–Al joints using CR model and OES measurements[J]. Plasma Science and Technology, 2023, 25(11): 115503. DOI: 10.1088/2058-6272/acddb7 |
In this study, we employed a non-invasive approach based on the collisional radiative (CR) model and optical emission spectroscopy (OES) measurements for the characterization of gas tungsten arc welding (GTAW) discharge and quantification of Zn-induced porosity during the GTAW process of Fe–Al joints. The OES measurements were recorded as a function of weld current, welding speed, and input waveform. The OES measurements revealed significant line emissions from Zn-Ⅰ in 460–640 nm and Ar-Ⅰ in 680–800 nm wavelength ranges in all experimental settings. The OES coupled CR model approach for Zn-Ⅰ line emission enabled the simultaneous determination of both essential discharge parameters i.e. electron temperature and electron density. Further, these predictions were used to estimate the Zn-induced porosity using OES-actinometry on Zn-Ⅰ emission lines using Ar as actinometer gas. The OES-actinometry results were in good agreement with porosity data derived from an independent approach, i.e. x-ray radiography images. The current study shows that OES-based techniques can provide an efficient route for real-time monitoring of weld quality and estimate porosity during the GTAW process of dissimilar metal joints.
Optical emission spectroscopy (OES) is a technique that records the intensity as a function of wavelength from a radiating source [1]. By analyzing the recorded spectrum, one can probe the chemical composition and physical properties of the radiating source. One of the significant benefits of OES is that it is non-invasive, and the measurements are straightforward [2]. Therefore, OES based approaches are being intensively used by the researchers. It is helpful in understanding the fundamental physics in driving the plasma and optimizing the plasma-mediated processing in a given application [3]. However, OES measurements are often required to be coupled with suitable population-kinetic models to extract the essential parameters, viz., electron temperature
In recent years, the need for welding different or dissimilar materials has increased to enhance material strength and durability while decreasing material weight [4]. The joining of various materials has been employed in various sectors, including the automobile, aerospace, nuclear power, and shipbuilding industries. However, creating a suitable joint between different metals can be challenging due to their distinct physical and chemical properties [5]. One solution that has gained popularity is the use of Fe–Al weld joints, or hybrid material joints, which can reduce the overall weight of products while maintaining strength and durability. These joints can be produced using various welding processes, such as gas tungsten arc welding (GTAW) and gas metal arc welding [5–8].
Despite their potential benefits, the application of zinc-based coatings on steel and the presence of surface impurities can contribute to a range of defects in the welding process [9]. These defects must be monitored to assess the quality of the weld. Porosity defects, or the presence of pores in the weld, can be particularly problematic during the post-weld inspection. Porosity defects can weaken the strength and integrity of the weld joint. Therefore it is essential to understand and quantify the porosity defects to optimize the GTAW processes [10].
In this light, various approaches, such as adjusting welding parameters, using different filler materials, and improving material cleanliness, were investigated [11, 12]. Often, internal porosity is detected post-welding through x-ray-based techniques, such as radiographic testing and 3D computed tomography (CT) [13]. These methods are time-consuming and can increase the cost of welding. Further, numerical modeling approaches have been adopted by a few researchers to address the porosity in weldments. Computational fluid dynamic (CFD) analysis helps in understanding the characteristic flow of the weld pool and predicting the porosity in the welding processes [14, 15]. These numerical models are computationally expensive and are proposed for porosity due to keyhole in the laser welding but not for the porosities induced by different vapors like Zn vapor. The results of welding simulations are often validated with experimental tests, but these tests can have uncertainties that make it challenging to debug [10]. Overall, the existing non-destructive testing methods or CFD-based models are not suitable for real-time monitoring and fast detection of defects during the welding operation.
In the present paper, we have employed the OES cum CR model based technique for the characterization of GTAW discharge and the quantification of Zn-induced porosity during the GTAW process of the Fe–Al joints. In this regard, the OES based methods can be very effective. Toropchin et al [12] used OES measurements to investigate the effect of arc temperature on weld pool behavior by conducting experiments with different currents, electrode-to-workpiece distances, and nozzle diameters. Goett et al [16] employed a combination of high-speed imaging and spatially resolved high-speed spectroscopy with a frame rate of up to 5000 fps to estimate the arc temperature in submerged arc welding. Mirapeix et al [17] have established a link between the
To the best of our knowledge, the use of OES in combination with a collisional radiative (CR) model and actinometry to understand and control defects arising from dissimilar metal joints has not been extensively studied. In the present work, we have investigated the role of Zn vapor in forming porosity during GTAW of Fe–Al joints. OES measurements were performed under various operating conditions, such as weld current, welding speed, and input waveform. The intensity line ratio of Zn to Ar (Ar serving as an actinometer gas) was used in conjunction with suitable theoretical modeling to determine the Zn population and its correlation with defects observed in the weld pool across the range of experimental parameters. These results were in good agreement with porosity data obtained from x-ray radiography images. This research highlights the potential of spectroscopic diagnostics as a valuable tool for quality control in the GTAW process of dissimilar metal joints. It demonstrates the ability to monitor weld quality, detect porosity defects, and estimate porosity levels during arc welding. This approach can be extended to other application areas. For example, it can be employed to assess quality control and monitor defects in additive manufacturing, ensuring the structural integrity of fabricated parts.
The experimental setup used in the present work is shown in figure 1. It consists of the Fronius make Magicwave 4000 arc plasma power supply, LEM make LF-310 S hall sensor, and Photron NOVA high-speed camera. The online recording of current and voltage waveforms is done with Dewesoft make data acquisition system. The arc images are synchronized with the instantaneous welding current and voltage waveforms at a sampling rate of 20 kHz. The typical arc images and respective temporal behavior of arc current are shown in figure S1 of the supplementary data. A bandpass filter (690 ± 10 nm) is used with high-speed camera to eliminate the arc light interference. The 1 mm thin sheets of AA6061-T6 aluminum alloy (Al) and galvannealed steel (Fe) of length 200 mm, width 100 mm are joined in lap joint configuration using AA4043 filler wire of 1.2 mm diameter. The detailed chemical composition of the materials is given in table S1 of the supplementary data. A non-corrosive Nocolok flux is applied uniformly at the brazing interface to improve the wetting of molten filler metal with the Fe sheet surface. Figure 1 depicts the joint configuration and setup used in joining Fe–Al sheets. The Fe and Al sheets are clamped on a fixture to restrict the distortions, keeping the Fe sheet at the bottom and maintaining an overlapping length of 15 mm. The fixture is mounted on a modular plate that moves at a given travel speed. Fe and Al sheets are degreased and cleaned using acetone before mounting on the fixture.
In the present work, the OES measurements are carried out under various joining conditions by varying the weld current, waveform, and joining speed, as mentioned in table 1. It is worth mentioning that small fluctuations in power are observed at constant current when the waveform is varied. We have performed calculations to determine the power from current–voltage measurements shown in figure S1 of the supplementary document for all the waveforms used in the experiment and determined the variation in the power. The results presented in table 1, indicate that the variation in power did not exceed 20−25 W, which is less than 5% of the average input power. We believe this variation is within the acceptable range. It is worth mentioning that in the GTAW process, the arc plasma is relatively more transient in nature. Therefore, performing the experiment with constant power results in a less stable arc, inconsistent weld penetration, and poor weld quality. In contrast, a constant current provides a stable welding current, even in the face of changes in arc length or electrode-to-work distance, which is essential for achieving high-quality GTAW welds. Thus, keeping constant current is a preferable choice without significant power fluctuations. Normally, if the power fluctuations are within 10% values, one can safely assume that input power is stable within the acceptable limit. In our experiment, we used a constant current power supply, specifically the Fronius Magicwave 4000 arc plasma power supply. This power supply is designed to provide a stable welding current, which allows for precise control over the heat input. We also fixed the sample to electrode tip distance, which helps in maintaining a constant voltage. This, in turn, helps to keep the power relatively constant.
Joining conditions | Weld current (A) | Joining speed (mm min–1) | AC waveform (power at 55 A) |
A1, A2, A3 | 50, 55, 60 | 120 | Square |
B1, B2, B3 | 55 | 90, 120, 150 | Square |
C1, C2, C3 | 55 | 120 | Square (594.89 ± 5 W), sine (610.38 ± 2 W), triangle (628 ± 4 W) |
The details of the operating conditions that were kept constant are given in table S2 of the supplementary data. The OES measurements are recorded using a spectrometer (Ocean-HDX-UV-VIS, Ocean Optics, Inc. USA) with a resolution (full width at half maxima) of 0.7 nm at a fixed position 50 cm away from the arc region. The OES measurement exhibits significant line emission from Zn Ⅰ in the region of 400−650 nm and Ar Ⅰ in the region of 680−800 nm, as shown in figures 2(a) and (b). The respective spectroscopic parameters of these emission lines are mentioned in tables S3 and S4 of the supplementary document. Typical arc emission spectra in the entire investigating wavelength range are shown in figure S2 of the supplementary document. The emissions due to Na Ⅰ and Mg Ⅰ at 589.2 nm and 518.5 nm are also observed due to the traces of these elements in the filler material. All the OES measurements are corrected for background noise and spectral response of the spectrometer. The OES measurements are repeated multiple times to estimate the possible uncertainties in the extracted plasma parameters.
In the present work, we employed an OES cum CR model based approach that can simultaneously estimate the electron temperature
To extract plasma parameters from OES measurements, we considered a CR model consisting of 31 fine-structure energy levels. As shown in the CR model framework in figure 3, energy levels corresponding to 4s4p, 4s5s, 4s5p, 4s4d, 4s6s, 4s6p, 4s5d, 4s7s, manifold along with ground state, and the first Zn+ ion state are considered. The population density of any fine-structure level of the CR model can be estimated by numerically solving the set of coupled balance rate equations. These rate balance equations are developed by incorporating major kinetic processes of the discharge, such as electron impact excitation/ionization, electron impact de-excitation, three-body recombination, spontaneous radiative decay, and quenching of metastable states. Following the CR model framework presented in figure 3, the rate balance equation for a given fine-structure level can be expressed as
dndt=31∑i=1,i≠fkexcitationif(Te)nine+∑i>fAifni+nen+nek+f(Te)−31∑i=1,i≠fkde−excitationfi(Te)nfne−∑i<fAfinf−nenfkf+(Te). | (1) |
These coupled rate balance equations are solved, assuming the steady state condition. In this equation,
kexcitationif=∫∞Eifσexcitationif(E)√Ef(E)dE. | (2) |
In this expression,
The current CR model differs from the previous model in which it incorporates the self-absorption of emission lines. We observed that including self-absorption is crucial in the present investigation conditions. Self-absorption is a phenomenon that occurs in practically all types of radiation sources, in which the strength of specific emission lines is reduced due to radiation absorption by the source itself. This can have an impact on the accuracy of the extracted plasma parameters. In the present work, we used an internal reference line-based approach proposed by Sun et al [25]. To accurately estimate the self-absorption correction factor, one should select the reference emission line that has a lower transition probability and a higher energy gap between its transition levels. The self-absorption correction coefficient (SACF) of emission lines using the following equation:
fbλ=IfiλImnλRAmngmAfigfe(Ef−Em/kBT), | (3) |
where,
The solution of CR model equations provides the population density of various levels as a function of input parameters
Δ=4∑j=1(INormalisedj,(OES)−INormalisedj,(Model))2. | (4) |
The
The zinc vapor density during the welding process is quantified using the line ratio of Zn Ⅰ and Ar Ⅰ emission lines. These line ratios are linked to the density of respective gas atoms. If the density of one gas atom (actinometer gas) is known, the other atom's density can be estimated. The actinometry method is widely used and extensively documented in the literature, so only a brief overview will be provided here [28, 29]. Assuming that respective excited states (from which the emission line originates) are mainly populated through electron-impact excitation and decay of these levels is by spontaneous emission, then the line ratio IZn/IAr can be given as [28]
IZnIAr=BZnkexcitationZn[nZn]BArkexcitationAr[nAr], | (5) |
where
To cross-validate the present zinc-induced porosity results in Al–Fe weld joints, results are compared with an independent approach based on x-ray computed tomography imaging. This technique allowed us to obtain a non-destructive, three-dimensional (3D) view of the weld and quantify any defects that may have occurred during the welding process [10]. The sample was placed on a rotating turntable between the x-ray source and detector, and x-rays were passed through the sample. These x-rays either passed through the sample or were attenuated, resulting in a gray-scale radiograph on the detector screen. The resolution of the scan was determined by the magnification factor of the object, which was influenced by the relative position of the x-ray source and detector. We acquired multiple radiographic projections through a full 360° rotation, which are then back-projected to reconstruct the image.
From the CR model, the level populations are obtained as a function
Figure 5(a) shows an increasing behavior of
Regarding the electron density
Further, the Ar-Ⅰ line ratio approach is utilized to estimate the qualitative behavior of
Tesensitivityratio=I763.5nmI738.3nm | (6) |
nesensitivityratio=I706.7nmI750.3nm. | (7) |
The results presented in figures 6(a) and (b) clearly show that the sensitive ratio of
Employing the plasma OES-actinometry technique, the qualitative behavior of Zn vapor density induced in the arc plasma welding process is investigated under various operating conditions, as mentioned in table 1. As evident from equation (5), the actinometry approach is directly linked with the emission line ratios. Figure 7 depicts the three-line ratios viz. 468.0 (Zn-Ⅰ)/750.3 (Ar-Ⅰ), 472.2 (Zn-Ⅰ)/750.3 (Ar-Ⅰ), and 481.0 (Zn-Ⅰ)/750.3 (Ar-Ⅰ). Figure 7(a) shows that the Zn-to-Ar increases with the weld current. Similarly, figure 7(b) shows that the Zn-to-Ar ratios decrease with joining speed. In the case of variation in input waveform, we can observe a significant rise in the intensity ratio from square waveform to triangle waveform. Further utilizing these ratios, the Zn-to-Ar population density ratio
As shown in figure 8, the Zn population increases almost linearly with the weld current. It is reasonable as
In our earlier investigation for heat generation with waveform variation, arc images indicate that the most intense arc occurs during the negative cycle of the triangle waveform, followed by the sine and square waveforms as shown in figures S1(a)–(c) of the supplementary document [8]. A similar trend can be seen in the extracted
To cross-verify plasma-actinometry results, the predicted Zn population density from OES-actinometry is compared to porosity data derived from an independent approach based on x-ray radiography images for operating conditions C1, C2, and C3 of table 1. Figure S4 shows the Fe–Al joint weld bead and their corresponding 3D CT scan images for conditions C1, C2, and C3, respectively. Figure 9 shows the size and number of porosities in the corresponding Fe–Al joints for conditions C1, C2, and C3, respectively, using the rendering technique of the graphics software. It is clear from the image that the size and number of porosities are significant for the triangle waveform, followed by the sine waveform. It is the least with the square waveform. The porosity in the weld bead is in trend with the population ratio. In the plasma environment, a higher Zn population is expected to introduce more Zn porosities in the weld bead. Such as for square waveform, Zn population is minimum, and the porosity is also negligible. Likewise, for the triangle waveform, the porosity size and number are maximum, and so is the Zn vapor population density.
The objective of this study was to investigate and observe the Zn induced porosity variation using spectroscopic diagnostics during the GTAW process. The following conclusions can be drawn from the present study:
(1) The Zn population is estimated for Fe–Al weld joints as a function of various experimental parameters such as weld current, joining speed, and input waveform.
(2) It is observed that there is a significant decrease in the zinc population ratio for low currents and joining speeds. In case of waveform, square waveform gives less zinc presence in arc compared to sine and triangle ones.
(3) For variation in AC waveforms the results are correlated with the 3D CT scan images, which agrees with the present model prediction. From figure S1, we can understand that as the peak currents increase, the arc diameter increases, which results in spiking zinc population density in the weld pool.
(4) Spectroscopic diagnostics, such as OES, can be a very effective non-destructive tool for real-time weld quality monitoring.
In conclusion, the present work demonstrates that OES is an efficient and fast method for estimating porosity during the GTAW process of Fe–Al joints. This present approach can also be employed in other areas, such as additive manufacturing, to assess structural integrity and defect detection in fabricated parts.
SS is thankful to the Ministry of Human Resources and Development (MHRD), Government of India, for providing HTRA fellowship. The authors gratefully acknowledge the support by the SERB, India, for listed Grants (Nos. CRG/2018/000419, CVD/2020/000458, and SB/S2/RJN-093/2015) Core Research Grant, India (No. CRG/2020/005089) and IIT Tirupati, India (No. MEE/18-19/008/NFSG/DEGA).
Supplementary material for this article is available https://doi.org/10.1088/2058-6272/acddb7
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Joining conditions | Weld current (A) | Joining speed (mm min–1) | AC waveform (power at 55 A) |
A1, A2, A3 | 50, 55, 60 | 120 | Square |
B1, B2, B3 | 55 | 90, 120, 150 | Square |
C1, C2, C3 | 55 | 120 | Square (594.89 ± 5 W), sine (610.38 ± 2 W), triangle (628 ± 4 W) |