Effect of Cr<sub>2</sub>O<sub>3</sub> nanosheet insertion on the deuterium permeation behavior of a Cr-Zr-O coating

Xinluo TIAN; Heping LI; Liyu ZHENG; Fangjian LI; Zhongyang ZHENG; Shengming YIN; Xinyun WANG; Youwei YAN

doi:10.1088/2058-6272/aca7ae

Plasma Science and Technology > 2022 > 24(12): 124017. > DOI: 10.1088/2058-6272/aca7ae

Xinluo TIAN, Heping LI, Liyu ZHENG, Fangjian LI, Zhongyang ZHENG, Shengming YIN, Xinyun WANG, Youwei YAN. Effect of Cr₂O₃ nanosheet insertion on the deuterium permeation behavior of a Cr-Zr-O coating[J]. Plasma Science and Technology, 2022, 24(12): 124017. DOI: 10.1088/2058-6272/aca7ae

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Effect of Cr₂O₃ nanosheet insertion on the deuterium permeation behavior of a Cr-Zr-O coating

State Key Laboratory of Materials Processing and Die & Mould Technology, International Joint Research Laboratory of Magnetic Confinement Fusion and Plasma Physics, School of Materials Science and Engineering, Huazhong University of Science and Technology, Wuhan 430074, People's Republic of China

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Corresponding author:
Heping LI, E-mail: liheping@hust.edu.cn
Received Date: August 12, 2022
Revised Date: November 29, 2022
Accepted Date: November 29, 2022
Available Online: December 05, 2023
Published Date: December 19, 2022

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Abstract

Abstract

In this study, a Cr₂O₃ nanosheet (Cr₂O₃ NS) inserted Cr-Zr-O coating was developed as a hydrogen isotope permeation barrier. The Cr₂O₃ NSs, fabricated by rapid heat treatment, were amorphous with a thickness of only several nanometers. These Cr₂O₃ NSs were then incorporated into a Cr-Zr-O multi-metal oxide composite coating via a dip-coating method to form a coating. The effect of the Cr₂O₃ NS concentration on the morphology, microstructure and deuterium permeation resistance of the coating was studied. With the addition of 1.0 g l^-1 Cr₂O₃ NSs, compared with the Cr-Zr-O coating without NSs, the permeation reduction factor of the resultant coating was enhanced from 249 ℃ to 575 ℃ at 500 ℃. The coating, with a thickness of nearly 193 nm, achieved a comparable deuterium resistance that was above two orders of magnitude higher than the steel substrate. The results show that ceramic NSs can serve as effective fillers for enhancing the coating performance when functioning as a hydrogen isotope barrier.
- deuterium permeation barrier,
- ceramic coatings,
- nanosheets

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Acknowledgments

This work was supported by the National MCF Energy R & D Program of China (No. 2018YFE0313300), National Natural Science Foundation of China (Nos. 52273224, 51402116), and the Fundamental Research Funds for the Central Universities (Nos. 2018KFYYXJJ028, 2019KFYXMBZ045). The authors thank the Analytical and Testing Center of Huazhong University of Science and Technology for their support.

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Effect of Cr₂O₃ nanosheet insertion on the deuterium permeation behavior of a Cr-Zr-O coating

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