Remote open-path laser-induced breakdown spectroscopy for the analysis of manganese in steel samples at high temperature

Minchao CUI (崔敏超); Yoshihiro DEGUCHI (出口祥啓); Zhenzhen WANG (王珍珍); Seiya TANAKA (田中诚也); Min-Gyu JEON (全敏奎); Yuki FUJITA (藤田裕贵); Shengdun ZHAO (赵升吨)

doi:10.1088/2058-6272/aaeba7

Plasma Science and Technology > 2019 > 21(3): 34007-034007. > DOI: 10.1088/2058-6272/aaeba7

Minchao CUI (崔敏超), Yoshihiro DEGUCHI (出口祥啓), Zhenzhen WANG (王珍珍), Seiya TANAKA (田中诚也), Min-Gyu JEON (全敏奎), Yuki FUJITA (藤田裕贵), Shengdun ZHAO (赵升吨). Remote open-path laser-induced breakdown spectroscopy for the analysis of manganese in steel samples at high temperature[J]. Plasma Science and Technology, 2019, 21(3): 34007-034007. DOI: 10.1088/2058-6272/aaeba7

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Remote open-path laser-induced breakdown spectroscopy for the analysis of manganese in steel samples at high temperature

¹ School of Mechanical Engineering, Xi’an Jiaotong University, Xi’an 710049, People’s Republic of China
² Graduate School of Advanced Technology and Science, University of Tokushima, Tokushima 770-8501, Japan
³ State Key Laboratory of Multiphase Flow in Power Engineering, Xi’an Jiaotong University, Xi’an 710049, People’s Republic of China
⁴ Division of Mechanical Engineering, Korea Maritime and Ocean University, Busan 49112, Republic of Korea

Funds: This work was supported by National Natural Science Foundation of China (Nos. 51506171 and 51675415), National Natural Science Foundation of China for Key Program (No. 51335009), National Key Research and Development Program of China (No. 2017YFD0700200) and the joint research fund between Tokushima University and Xi’an Jiaotong University.

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Received Date: August 29, 2018

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Abstract

Abstract

A remote open-path laser-induced breakdown spectroscopy (LIBS) system was designed and studied in the present work for the purpose of combining the LIBS technique with the steel production line. In this system, the relatively simple configuration and optics were employed to measure the steel samples at a remote distance and a hot sample temperature. The system has obtained a robustness for the deviation of the sample position because of the open-path and all- optical structure. The measurement was carried out at different sample temperatures by placing the samples in a muffle furnace with a window in the front door. The results show that the intensity of the spectral lines increased as the sample temperature increased. The influence of the sample temperature on the quantitative analysis of manganese in the steel samples was investigated by measuring ten standard steel samples at different temperatures. Three samples were selected as the test sample for the simulation measurement. The results show that, at the sample temperature of 500°C, the average relative error of prediction is 3.1% and the average relative standard deviation is 7.7%, respectively.
- remote,
- open-path,
- LIBS,
- steel,
- manganese,
- sample temperature,
- quantitative analysis

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References (35)

References

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Remote open-path laser-induced breakdown spectroscopy for the analysis of manganese in steel samples at high temperature